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Accuracy of the proposed method was assessed with spiking experiments performed on complex sample matrices. Percent recoveries calculated for spiked soil, artificial seawater and seaweed samples were in acceptable ranges of 95 - 121%, 87 - 117% and 85 - 111%, respectively. These figures of merit suggest that HPLC-UV coupled with the US-Fe3O4@rGO-DSPEmethod is suitable for the determination of parabens in Antarctic samples.The design and development of materials with a selective adsorption capacity for Pb(II) are very important for envi