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This work clarifies the role of surface defects and the significance of their passivation to prevent hydration and decomposition reactions.Quantitative chemical analysis on the nanoscale provides valuable information on materials and devices which can be used to guide further improvements to their performance. In particular, emerging families of technologically relevant composite materials such as organic-inorganic hybrid halide perovskites and metal-organic frameworks stand to benefit greatly from such characterization. However, these
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