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In this research, the treatment of methylene blue (M dye wastewater by a novel system that combines H2O2 with an aluminum-carbon micro-electrolysis (ACE) was explored. The effects of the H2O2 amount, initial pH, aluminum to carbon ratio, total aluminum-carbon mass, dye concentration, and reaction temperature on degradation of MB were investigated. The findings revealed that under the following conditions H2O2 34.0 mg/L, initial pH of 3.0, aluminum-to-carbon ratio of 21, total aluminum-carbon mass of 2.0 g/L, MB concentration of 20 mg/L
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