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The architectural, morphological, thermal, and electrochemical properties of antimonene had been comparatively reviewed against bulk antimony. X-ray diffractometry (XRD) analysis confirms the crystal framework and 2D framework of antimonene, as a peak change had been observed. The Raman spectra show the peak shift when it comes to Eg and A1g modes of vibration of antimony, which confirms the forming of antimonene. Scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM) pictures depict the exfolia