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In this study, char was prepared from the Şırnak coal derivative as a new adsorbent by the pyrolysis process and successfully applied for Pb (II) removal. Prepared char adsorbent was characterized by analysis techniques such as thermogravimetric (TG)/differential thermogravimetric (DTG), iodine number, scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-IR), and Brunauer-Emmett-Teller (BET) surface area. In the experimental design of the Pb (II) removal process, the relationship between operating factors (con