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Layered covalent-organic frameworks (2D-COFs), composed of reversible imine-linkages and accessible pores, offer a versatile platform for chemical modifications towards the development of catalytic materials. Notably, nitrogen-enriched COF materials have been proved as good candidates for binding palladium species. Understanding the local structure of reacting palladium sites bonded to the COF pores is key to rationalize interactions between active sites and porous surfaces. By combining advanced synchrotron characterization tools, such a
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