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In this study, persulfate was used during hydrothermal processing of spirulina (160℃-220℃) for enhancement of nitrogen conversion. The nitrogen distribution in aqueous phase, hydrochar and biocrude-oil was evaluated, and the elemental composition and chemical forms of hydrochar were investigated. Results suggested that the addition of persulfate during hydrothermal processing of spirulina increased the atomic N/O of hydrochar for 1.2%-2.4%, whereas the NH4+-N concentration in liquid phase increased by approximately 67-155 mg/L regardles