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La3+-2D-g-C3N4 shows the photodegradation efficiency (93%) of ciprofloxacin under UV irradiation, which is superior to pristine 2D-g-C3N4 (82%) as well as other g-C3N4 based nanocatalysts. Also, La3+ decoration results in enhancement (32.3%) in photodegradation kinetics rate. The degradation and kinetics studies in the presence of different scavengers ensure that the O2- and OH- radicals are mostly responsible for the ciprofloxacin photodegradation. The Liquid chromatographic-mass spectroscopy and the high-performance liquid chromatogra