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MoAlB item particles exhibited various shapes/sizes, as follows spherical grains (1~3 μm), plate-like particles ( less then 5 μm in diameter) and columnar crystals with lengths as much as 20 μm and diameters as much as 5 μm, resultant from various response procedures. Phase pure MoAlB was synthesised under the after ideal conditions use of 140% extra Al and 6 h of firing at 1000 °C. This heat is at minimum 100 °C less than required by various