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The results show that LIBS assisted with molecular synthesis has a huge potential in water quality monitoring.In this study, the successful coupling of a 3D printed electrochemical flow cell and online multi-element analysis by ICP-OES is presented. The feasibility of the coupled method is investigated on the basis of hot-dip coated steel sheet dissolution in diluted HCl (20%). At first a qualitative evaluation of the electrochemical and element information of the coated steel substrate and relating the results to a glow-discharge optica