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Interface manufacturing and plasma-assisted problems regarding the p-n Cox Ni3-x (HITP)2 /BNSs-P heterojunction led to the development of both Co-N3 and B…O dual-active websites. Because of this, Cox Ni3-x (HITP)2 /BNSs-P has a high NH3 yield of 128.26 ± 2.27 µg h-1 mgcat. -1 and a Faradaic efficiency of 52.92 ± 1.83% in 0.1 m HCl answer. The catalytic procedure for the eNRR is also studied by in situ FTIR spectra and DFT calculations. A Cox Ni3- x (HITP)2 /BNSs-P-based Zn-
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