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This approach provides an innovative method for the large-scale production and application of high-quality catalysts in water treatment. To enhance the photocatalytic activity of TiO2, a new preparation method has been proposed to synthesize the catalysts by introducing Cu-MOF as a precursor and performing a blackening process via a mixture with NaBH4 for TiO2 nanoparticles (CuO-TiO2(mb)). The results showed that the removal efficiency of xylene under ultraviolet and visible light over CuO-TiO2(mb) was 3.45 times higher than that of the ca